Ag_2Se纳米晶的水热合成及表征Hydrothermal synthesis and characterization of Ag_2Se nanocrystals
金盈,吴友吉,吴之传,陈玉村
摘要(Abstract)：
在低温水热条件下,以AgNO3、Na2SeO3或单质硒为反应物,制备了金属硫族化合物Ag2Se纳米晶.用X射线粉末衍射(XRD)、透射电镜(TEM)、扫描电镜(SEM)分别对Ag2Se纳米晶的结构及形貌进行了表征分析.结果表明,所得样品为正交晶系的Ag2Se纳米晶,主要形貌为不规则的纳米颗粒;同时采用不同硒源及表面活性剂聚乙烯吡咯烷酮(PVP)可以获得不同形貌的纳米晶.
关键词(KeyWords)： 水热合成;Ag2Se纳米晶;表面活性剂
基金项目(Foundation): 安徽省教育厅科研基金资助项目(2004kj034zd);; 安徽工程科技学院青年基金资助项目(2003YQ003)
作者(Author): 金盈,吴友吉,吴之传,陈玉村
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